Benzylamine → N-[5-(2-Phenylethoxy)pentyl]benzenemethanamine

反応式

Br[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][O:7][CH2:8][CH2:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1.[CH2:16]([NH2:23])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>>[C:10]1([CH2:9][CH2:8][O:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][NH:23][CH2:16][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1

参加物

反応物 2

HCID 7504Benzylamine

HCID 197980262-(5-Bromopentoxy)ethylbenzene

生成物 1

HCID 20062790N-[5-(2-Phenylethoxy)pentyl]benzenemethanamine

実験手順

N-[5-(2-Phenylethoxy)pentyl]benzenemethanamine (8.6 g) was prepared in a similar manner from [2-[(5-bromopentyl)oxy]ethyl]benzene (10 g) and benzylamine (30 ml). The undistilled product was used without further purification in Example 1(c).

後処理

distillationThe undistilled product was used without further purification in Example 1(c)

出典と根拠

ORDレコード: ord-6f7a477d80444cfebad50c1f20fadd40
出典データセット: uspto-grants-1990_07
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04943591

反応ノート

読み込み中…