1H-1,2,4-Triazole → 4-[2-(1H-1,2,4-Triazol-1-yl)ethyl]phenol

反応式

[NH:1]1[CH:5]=[N:4][CH:3]=[N:2]1.C([O:13][C:14]1[CH:19]=[CH:18][C:17]([CH2:20][CH2:21]OS(C)(=O)=O)=[CH:16][CH:15]=1)C1C=CC=CC=1>>[N:1]1([CH2:21][CH2:20][C:17]2[CH:18]=[CH:19][C:14]([OH:13])=[CH:15][CH:16]=2)[CH:5]=[N:4][CH:3]=[N:2]1

参加物

反応物 2

HCID 92571H-1,2,4-Triazole

HCID 115004941-Benzyloxy-4-(2-methanesulfonyloxyethyl)benzene

生成物 1

HCID 202052954-[2-(1H-1,2,4-Triazol-1-yl)ethyl]phenol

実験手順

In a manner analogous to that described in Example 10(b), from 1H-1,2,4-triazole and 1-benzyloxy-4-(2-methane-sulfonyloxyethyl)benzene, 4-[2-(1H-1,2,4-triazol-1-yl)ethyl]phenol was obtained.

出典と根拠

ORDレコード: ord-e57935d9e4f6480f8a788cb35c2f38bb
出典データセット: uspto-grants-1983_06
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04387100

反応ノート

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