化工社化工社 化学情報印刷レポート · 研究参考用
1,4-Dibromobutane → 1-(4-Chlorophenyl)cyclopentanecarbonitrile
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,4-Dibromobutane | HCID 8056 | — |
| 反応物 | 1-Phenylcyclopentanecarbonitrile | HCID 66168 | — |
| 反応物 | 4-Chlorobenzyl cyanide | HCID 241582 | — |
| 生成物 | 1-(4-Chlorophenyl)cyclopentanecarbonitrile | HCID 97384 | 94% |
反応手順
1-(4-chlorophenyl)-cyclopentanecarbonitrile (21-02) (32.01 g, 94%) was synthesized as a yellow liquid from (4-chlorophenyl)-acetonitrile (19-02) (25 g, 165.56 mmol) and 1,4-dibromo-butane (20) (19.7 mL, 165.56 mmol) following the procedure as described for 1-phenyl-cyclopentanecarbonitrile (21-01).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09045486B2 |
| 出典データセット | uspto-grants-2015_06 |
| ORD ID | ord-fde9c76ba284485cbe2a9ba05fc27aea |
| 出典メモ | uspto-grants-2015_06 |