化工社化工社 化学情報印刷レポート · 研究参考用
1-(p-Chlorophenyl)cyclopentanemethanol → Methanesulfonic acid 1-(4-chlorophenyl)-cyclopentylmethyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-(p-Chlorophenyl)cyclopentanemethanol | HCID 2724017 | — |
| 反応物 | (1-Phenylcyclopentyl)methyl methanesulfonate | HCID 19437914 | — |
| 生成物 | Methanesulfonic acid 1-(4-chlorophenyl)-cyclopentylmethyl ester | HCID 86725805 | 93.08% |
反応手順
Methanesulfonic acid 1-(4-chlorophenyl)-cyclopentylmethyl ester (24-02) (32 g, 93.08%) was synthesized from [1-(4-chlorophenyl)-cyclopentyl]-methanol (23-02) (25 g, 119.04 mmol) as a crude product as a yellow liquid following the procedure as described for methanesulfonic acid 1-phenyl-cyclopentylmethyl ester (24-01).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09045486B2 |
| 出典データセット | uspto-grants-2015_06 |
| ORD ID | ord-16ed389b6b5945cd914b15602d2a9074 |
| 出典メモ | uspto-grants-2015_06 |