戻る
化工社化工社 化学情報印刷レポート · 研究参考用
HRID 2170240作成日:2026年10月26日

Resveratrol → 5-(2-(4-Hydroxyphenyl)Ethenyl)Benzene-1,3-Diol

https://huagongshe.com/reaction/2170240

反応式

関与物質

役割名称HCID仕込み量
反応物ResveratrolHCID 445154—
反応物Sodium BicarbonateHCID 516892—
溶媒EthanolHCID 702—
生成物5-(2-(4-Hydroxyphenyl)Ethenyl)Benzene-1,3-DiolHCID 5056—

反応手順

700 mg of trans-resveratrol (manufactured by Tokyo Chemical Industry Co., Ltd.) was dissolved in 14 ml of ethanol, and then 14 mL of a 2.5% NaHCO3 aqueous solution was added thereto to obtain a resveratrol containing solution (pH 9.9). The resveratrol containing solution was heated at 130° C. for 20 minutes in an autoclave (“SANYO LABO AUTOCLAVE” manufactured by SANYO Electric Co., Ltd., which was used in the following Examples). Subsequently, 14 ml of ethanol and 14 mL of a 5.0% NaHCO3 aqueous solution were added to the reaction solution obtained by the first autoclave treatment, and then heated again at 130° C. for 20 minutes in the autoclave. Then, 1 mL of the obtained reaction solution was diluted with methanol in a measuring cylinder to 50 mL, and then 10 L, thereof was analyzed by HPLC.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US09051245B2
出典データセットuspto-grants-2015_06
ORD IDord-74c3a81a4de34061a5520bedb7187f05
出典メモuspto-grants-2015_06