Suberic acid → Oxonane-2,9-dione
反応式
[C:1]([OH:12])(=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][C:8]([OH:10])=O>CC(OC(C)=O)=O>[O:12]1[C:1](=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][C:8]1=[O:10]参加物
3
試薬・触媒・溶媒 1
実験手順
Under N2 atmosphere 50 g suberic acid and 100 ml acetanhydride were refluxed for 2 hours. The solvent was evaporated and 200 ml acetonitrile were added to the residue and the mixture was kept in a freezer over night. Then the mixture was fritted and the resulting residue was washed with 50 ml acetonitrile and dried.
後処理
- customThe solvent was evaporated
- addition200 ml acetonitrile were added to the residue
- waitthe mixture was kept in a freezer over night
- washthe resulting residue was washed with 50 ml acetonitrile
- customdried
出典と根拠
- ORDレコード
- ord-d4634b1c94844c949baa8b06a896ae0b
- 出典データセット
- uspto-grants-2012_06
- 特許番号
- US08193246B2
反応ノート
読み込み中…