Potassium Hydroxide → HCID 67110796、化合物

反応式

[OH-].[K+:2].[C:3]([OH:15])(=[O:14])/[CH:4]=[CH:5]/[C:6]1[CH:13]=[CH:12][C:10]([OH:11])=[C:8](O)[CH:7]=1>>[OH:11][C:10]1[CH:8]=[CH:7][C:6]([CH:5]=[CH:4][C:3]([O-:15])=[O:14])=[CH:13][CH:12]=1.[K+:2]

参加物

反応物 2

HCID 14797Potassium Hydroxide

HCID 689043Caffeic Acid

生成物 1

HCID 67110796HCID 67110796、化合物

実験手順

To 15 mL of a 0.002 mM aqueous solution of potassium hydroxide was slowly added 5 g coumaric acid 190 (30 mmol) with mixing at 60-70° C. The resulting potassium coumarate (200) was dried under vacuum at 30-40° C.

後処理

additionwith mixing at 60-70° C
dry with materialThe resulting potassium coumarate (200) was dried under vacuum at 30-40° C.

出典と根拠

ORDレコード: ord-1d41f0d8a1a8418888275cf2436624cd
出典データセット: uspto-grants-2015_06
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US09061993B2

反応ノート

読み込み中…

参加物