Oxygen → 1-[3-(3,3-Dimethylbutoxy)-5-ethoxyphenyl]ethanone
反応式
[OH:1][C:2]1[CH:3]=[C:4]([C:9](=[O:11])[CH3:10])[CH:5]=[C:6]([OH:8])[CH:7]=1.O=O.[CH:14]1(Br)CCCC[CH2:15]1.Br[CH2:22][CH2:23][C:24]([CH3:27])([CH3:26])[CH3:25]>>[CH3:25][C:24]([CH3:27])([CH3:26])[CH2:23][CH2:22][O:1][C:2]1[CH:3]=[C:4]([C:9](=[O:11])[CH3:10])[CH:5]=[C:6]([O:8][CH2:14][CH3:15])[CH:7]=1参加物
5
実験手順
1-(3,5-Dihydroxyphenyl)ethanone (3.0 g) were converted analogously to O2.031. Instead of cyclohexylbromide, however, 1-bromo-3,3-dimethylbutane was used. After chromatography, 960 mg of the title compound were obtained.
出典と根拠
- ORDレコード
- ord-41bb97f56a5143b8a40ef754de57fc47
- 出典データセット
- uspto-grants-2012_06
- 特許番号
- US08198272B2
反応ノート
読み込み中…