Methyl 3-bromo-6-(3-chlorobenzenesulphonylmethyl)-2-hydroxybenzoate → Methyl 3-bromo-6-(4-fluorobenzenesulphonylmethyl)-2-hydroxybenzoate

HRID 2177728ノート

反応式

HRID 2177728 の反応式
BrC1C(O)=C(C(CS(C2C=CC=C(Cl)C=2)(=O)=O)=CC=1)C(OC)=O.[Br:24][C:25]1[C:26]([O:46]C)=[C:27]([C:32]([CH2:35][S:36]([C:39]2[CH:44]=[CH:43][C:42]([F:45])=[CH:41][CH:40]=2)(=[O:38])=[O:37])=[CH:33][CH:34]=1)[C:28]([O:30][CH3:31])=[O:29]>>[Br:24][C:25]1[C:26]([OH:46])=[C:27]([C:32]([CH2:35][S:36]([C:39]2[CH:40]=[CH:41][C:42]([F:45])=[CH:43][CH:44]=2)(=[O:38])=[O:37])=[CH:33][CH:34]=1)[C:28]([O:30][CH3:31])=[O:29]

参加物

3

反応物 2

HCID 67107545Methyl 3-bromo-6-(3-chlorobenzenesulphonylmethyl)-2-hydroxybenzoateHCID 67107935Methyl 3-bromo-6-(4-fluorobenzenesulphonylmethyl)-2-methoxybenzoate2 回

生成物 1

HCID 67107667Methyl 3-bromo-6-(4-fluorobenzenesulphonylmethyl)-2-hydroxybenzoate

実験手順

Prepared by proceeding in a similar manner to Intermediate 54, starting from methyl 3-bromo-6-(4-fluorobenzenesulphonylmethyl)-2-methoxybenzoate (Intermediate 69).

後処理

  1. customPrepared

出典と根拠

ORDレコード
ord-1db99f367a3844b6a76be57d7558bf3e
出典データセット
uspto-grants-2015_06
特許番号
US09067905B2

反応ノート

読み込み中…