Hydrazine → HCID 54275604、化合物

HRID 21807ノート

反応式

HRID 21807 の反応式
[NH2:1]N.[CH3:3][N:4]1[CH2:9][CH2:8][NH:7][CH2:6][CH:5]1[CH2:10][CH2:11][CH2:12][CH2:13]C1C=CC=C2C(NC(=O)C=12)=O>CO>[CH3:3][N:4]1[CH2:9][CH2:8][NH:7][CH2:6][CH:5]1[CH2:10][CH2:11][CH2:12][CH2:13][NH2:1]

参加物

4

反応物 2

HCID 9321HydrazineHCID 538263884-(N-methylpiperazinyl)butylphthalimide

生成物 1

HCID 54275604HCID 54275604、化合物

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 4-(N-methylpiperazinyl)butylphthalimide (240 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

後処理

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

出典と根拠

ORDレコード
ord-c944c58f544d4256941c6aa331ac25a9
出典データセット
uspto-grants-1995_06
特許番号
US05424451

反応ノート

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