Hydrazine → 8-Pyrrolidinyloctylamine

HRID 21813ノート

反応式

HRID 21813 の反応式
[NH2:1]N.[N:3]1([CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15]C2C=CC=C3C(NC(=O)C=23)=O)[CH2:7][CH2:6][CH2:5][CH2:4]1>CO>[N:3]1([CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][NH2:1])[CH2:4][CH2:5][CH2:6][CH2:7]1

参加物

4

反応物 2

HCID 9321HydrazineHCID 542934218-Pyrrolidinyloctylphthalimide

生成物 1

HCID 199335008-Pyrrolidinyloctylamine

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 8-pyrrolidinyloctylphthalimide (263 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

後処理

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

出典と根拠

ORDレコード
ord-57327deb27424964be85d1a8d0e252d6
出典データセット
uspto-grants-1995_06
特許番号
US05424451

反応ノート

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