Hydrazine → 8-Piperidinyloctylamine

HRID 21814ノート

反応式

HRID 21814 の反応式
[NH2:1]N.[N:3]1([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16]C2C=CC=C3C(NC(=O)C=23)=O)[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1>CO>[N:3]1([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][NH2:1])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]1

参加物

4

反応物 2

HCID 9321HydrazineHCID 540305088-Piperidinyloctylphthalimide

生成物 1

HCID 110092698-Piperidinyloctylamine

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 8-piperidinyloctylphthalimide (274 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

後処理

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

出典と根拠

ORDレコード
ord-e06d024b9acb4c0eadbd0144dfda4742
出典データセット
uspto-grants-1995_06
特許番号
US05424451

反応ノート

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