4-Chloro-2-hydroxybenzonitrile → HCID 131724957、化合物

反応式

[Cl:1][C:2]1[CH:9]=[CH:8][C:5]([C:6]#[N:7])=[C:4]([OH:10])[CH:3]=1.O[CH:12]([CH2:24][CH:25]([CH3:27])[CH3:26])[CH2:13][CH2:14][N:15]([CH3:23])[C:16](=[O:22])[O:17][C:18]([CH3:21])([CH3:20])[CH3:19]>>[CH3:21][C:18]([O:17][C:16](=[O:22])[N:15]([CH2:14][CH2:13][CH:12]([O:10][C:4]1[CH:3]=[C:2]([Cl:1])[CH:9]=[CH:8][C:5]=1[C:6]#[N:7])[CH2:24][CH:25]([CH3:26])[CH3:27])[CH3:23])([CH3:19])[CH3:20]

参加物

反応物 2

HCID 34427894-Chloro-2-hydroxybenzonitrile

HCID 91303071HCID 91303071、化合物

生成物 1

HCID 131724957HCID 131724957、化合物

実験手順

The title compound was prepared according to the method of Example 2 step (b) but using 4-chloro-2-hydroxybenzonitrile and (3-hydroxy-5-methylhexyl)methylcarbamic acid, 1,1-dimethylethyl ester.

出典と根拠

ORDレコード: ord-827794918c4a42dc8185462d39ba331b
出典データセット: uspto-grants-2005_05
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US06900243B2

反応ノート

読み込み中…