化工社化工社 化学情報印刷レポート · 研究参考用
Tri(2-ethylhexyl)amine → 5-Butoxy-4-methyl-1,3-oxazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Tri(2-ethylhexyl)amine | HCID 102705 | — |
| 反応物 | n-Butyl alpha-isocyanopropionate | HCID 11171108 | — |
| 溶媒 | Chlorobenzene | HCID 7964 | — |
| 生成物 | 5-Butoxy-4-methyl-1,3-oxazole | HCID 9877440 | — |
反応手順
A column according to example 1 but without a dividing wall (see FIG. 1) was continuously charged via inlet (A) with a mixture of 20.6% by weight of chlorobenzene, 5.2% by weight of n-butyl α-isocyanopropionate (R1=n-butyl, R2=methyl) and 72.60% by weight of tris(2-ethylhexyl)amine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06900332B2 |
| 出典データセット | uspto-grants-2005_05 |
| ORD ID | ord-312a9549597e4547b328fa5943b4196a |
| 出典メモ | uspto-grants-2005_05 |