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HRID 2184627作成日:2026年10月27日

Propylene Oxide → Propylene oxide butylene oxide

https://huagongshe.com/reaction/2184627

反応式

関与物質

役割名称HCID仕込み量
反応物Propylene OxideHCID 6378—
反応物Potassium HydroxideHCID 14797—
反応物DiglycerinHCID 42953—
溶媒TetrahydrofuranHCID 8028—
生成物Propylene oxide butylene oxideHCID 22138293—

反応手順

166 g of a starting substance, diglycerin, 32 g of a catalyst, potassium hydroxide, 9,290 g of propylene oxide, and 1,460 g of butylene oxide were put into a 15-L autoclave, and reacted at 110° C. for 16 hours, and then neutralized, desalted and purified to obtain 9,900 g of a tetra-functional propylene oxide-butylene oxide copolymer. This polymer had a molecular weight of 10,900 (as calculated from its hydroxyl value).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06399254B1
出典データセットuspto-grants-2002_06
ORD IDord-22fc703fc6ff4d6c990dbe51abac4b40
出典メモuspto-grants-2002_06