HCID 22458129、化合物 → HCID 11628605、化合物
反応式
[CH:1]1([C:7](N(C2C=CC=CC=2OC(F)(F)F)CCN2CCN(C3C=CC([N+]([O-])=O)=CC=3OC)CC2)=[O:8])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[F:40][C:41]([F:69])([F:68])[O:42][C:43]1[CH:48]=[CH:47][CH:46]=[CH:45][C:44]=1[NH:49][CH2:50][CH2:51][N:52]1[CH2:57][CH2:56][N:55]([CH2:58][C:59]2[CH:64]=[C:63]([O:65][CH3:66])[CH:62]=[CH:61][C:60]=2[Br:67])[CH2:54][CH2:53]1>>[CH:1]1([C:7]([N:49]([C:44]2[CH:45]=[CH:46][CH:47]=[CH:48][C:43]=2[O:42][C:41]([F:40])([F:68])[F:69])[CH2:50][CH2:51][N:52]2[CH2:57][CH2:56][N:55]([CH2:58][C:59]3[CH:64]=[C:63]([O:65][CH3:66])[CH:62]=[CH:61][C:60]=3[Br:67])[CH2:54][CH2:53]2)=[O:8])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1参加物
3
実験手順
The title compound was prepared following the procedure described for the compound of example 55, substituting the compound of example 74 for the compound of example 54. The residue was purified by flash chromatography (CHCl3-2 N methanolic NH3 100:1). Yield: 67%.
後処理
- customThe residue was purified by flash chromatography (CHCl3-2 N methanolic NH3 100:1)
出典と根拠
- ORDレコード
- ord-3b7c6cebbaee4174ae7c77b9ec424081
- 出典データセット
- uspto-grants-2002_06