HCID 18782313、化合物 → HCID 22458144、化合物
反応式
[C:1]([C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[N:9]([C:27]([CH:29]1[CH2:34][CH2:33][CH2:32][CH2:31][CH2:30]1)=[O:28])[CH2:10][CH2:11][N:12]1[CH2:17][CH2:16][N:15]([C:18]2[CH:23]=[CH:22][C:21]([NH2:24])=[CH:20][C:19]=2[O:25][CH3:26])[CH2:14][CH2:13]1)#[N:2].NC1C=CC=CC=1N(C(C1CCCCC1)=O)CCN1CCN([C:51]2C=CC=C[C:52]=2[O:57]C)CC1>>[C:1]([C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[N:9]([C:27]([CH:29]1[CH2:34][CH2:33][CH2:32][CH2:31][CH2:30]1)=[O:28])[CH2:10][CH2:11][N:12]1[CH2:13][CH2:14][N:15]([C:18]2[CH:23]=[CH:22][C:21]([NH:24][C:52](=[O:57])[CH3:51])=[CH:20][C:19]=2[O:25][CH3:26])[CH2:16][CH2:17]1)#[N:2]参加物
3
反応条件
- 温度
- 22.5 °C
実験手順
The title compound was synthesized according to the procedure reported in example 28 but substituting the compound of example 79 for the compound of example 27 and stirring at 20-25° C. for 17 h. The usual work-up afforded the title compound. Yield: 49%.
後処理
- customThe title compound was synthesized
出典と根拠
- ORDレコード
- ord-eba033b531a64b1ab9abd7f83f9783b8