Methanol → methyl (2S)-2,3-dihydro-1H-indole-2-carboxylate
反応式
[NH:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH2:3][C@H:2]1[C:10]([OH:12])=[O:11].[CH3:13]O>S(=O)(=O)(O)O>[NH:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH2:3][C@H:2]1[C:10]([O:12][CH3:13])=[O:11]参加物
4
実験手順
Indoline-2(S)-carboxylic acid (10 g, 64 mmol) was refluxed in a mixture of methanol (50 ml) and sulphuric acid (8 ml) for 5 h. The solvent was removed to give the product in the form of an oil.
後処理
- customThe solvent was removed
- customto give the product in the form of an oil
出典と根拠
- ORDレコード
- ord-e67c410ff18343e7a8bb2b621cca852e
- 出典データセット
- uspto-grants-2002_06
- 特許番号
- US06403561B1
反応ノート
読み込み中…