Tolylboronic acid → HCID 12659171、化合物
反応式
Br[C:2]1[S:3][C:4]2[CH:10]=[CH:9][C:8]([Cl:11])=[CH:7][C:5]=2[CH:6]=1.[CH3:12][C:13]1[CH:18]=[CH:17][C:16](B(O)O)=[CH:15][CH:14]=1>C(OCC)(=O)C>[Cl:11][C:8]1[CH:9]=[CH:10][C:4]2[S:3][C:2]([C:16]3[CH:17]=[CH:18][C:13]([CH3:12])=[CH:14][CH:15]=3)=[CH:6][C:5]=2[CH:7]=1参加物
4
実験手順
The compound was prepared in the same manner as described in Preparation 48, Step B, from 2.06 g (8.32 mmol) 2-bromo-5-chlorobenzothiophene and 2.44 g (17.95 mmol) 4-methylbenzeneboronic acid and isolated by crystallization from ethyl acetate.
後処理
- customThe compound was prepared in the same manner
出典と根拠
- ORDレコード
- ord-c3bd66f4ea874e078ff07dc2e86bf7b6
- 出典データセット
- uspto-grants-2002_06
- 特許番号
- US06410562B1
反応ノート
読み込み中…