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Methyl iodide → N,N-diethyl 2-chloro-6-methylbenzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl iodide | HCID 6328 | — |
| 反応物 | 2-Chloro-N,N-diethylbenzamide | HCID 82566 | — |
| 生成物 | N,N-diethyl 2-chloro-6-methylbenzamide | HCID 18630133 | 92% |
反応手順
The compound from example e (1.0 eq) and MeI (3.0 eq) were combined according to Method A. The crude product was purified by HPLC with 1:4 EtOAc/hexanes to give 5.2 g of N,N-diethyl 2-chloro-6-methylbenzamide as a yellow solid, a 92% yield. m.p. 48°-49° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06410558B1 |
| 出典データセット | uspto-grants-2002_06 |
| ORD ID | ord-6e4686cee83448fdaf5bb2bce7a792cc |
| 出典メモ | uspto-grants-2002_06 |