Ethylamine → HCID 67274438、化合物
反応式
[C:1]1([CH2:7][N:8]2[CH2:13][CH2:12][N:11]([CH2:14][C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=3)[CH2:10][CH:9]2[CH:21]=O)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:23]([NH2:25])[CH3:24]>ClCCl>[CH2:7]([N:8]1[CH2:13][CH2:12][N:11]([CH2:14][C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)[CH2:10][CH:9]1[CH:21]=[N:25][CH2:23][CH3:24])[C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1参加物
4
実験手順
To a solution of 0.5 g (1,4-bis(phenylmethyl)-2-piperazin-carboxaldehyde in 5 ml of dichloromethane was added 0.54 ml ethylamine and 0.5 g molecular sieves. The reaction mixture was stirred for 30 min at rt then filtered. The filtrate was evaporated to dryness.
後処理
- filtrationthen filtered
- customThe filtrate was evaporated to dryness
出典と根拠
- ORDレコード
- ord-4768627adb034e5dba895faf09162926
- 出典データセット
- uspto-grants-2012_12
- 特許番号
- US08329908B2
反応ノート
読み込み中…