2-(Trifluoromethoxy)benzene-1-sulfonyl chloride → HCID 59578089、化合物
反応式
C(O[C:4]([C:6]1([CH2:12][CH2:13]OC)[CH2:11][CH2:10][NH:9][CH2:8][CH2:7]1)=[O:5])C.[F:16][C:17]([F:30])([F:29])[O:18][C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][C:20]=1[S:25](Cl)(=[O:27])=[O:26].[CH3:31][O:32][CH2:33][C:34]([C:37]1[CH:42]=[CH:41][C:40]([NH2:43])=[CH:39][CH:38]=1)([CH3:36])[CH3:35]>>[CH3:31][O:32][CH2:33][C:34]([C:37]1[CH:38]=[CH:39][C:40]([N:43]2[CH2:13][CH2:12][C:6]3([CH2:7][CH2:8][N:9]([S:25]([C:20]4[CH:21]=[CH:22][CH:23]=[CH:24][C:19]=4[O:18][C:17]([F:30])([F:29])[F:16])(=[O:27])=[O:26])[CH2:10][CH2:11]3)[C:4]2=[O:5])=[CH:41][CH:42]=1)([CH3:36])[CH3:35]参加物
4
実験手順
Off-white crystalline solid. MS (ESI): 541.19 (MH+). This example was prepared in analogy to example 1 step C) to D) from 4-(2-methoxy-ethyl)-piperidine-4-carboxylic acid ethyl ester (example 1 step B)), 2-trifluoromethoxy-benzenesulfonyl chloride and 4-(2-methoxy-1,1-dimethyl-ethyl)-phenylamine.
出典と根拠
- ORDレコード
- ord-c704643484764d2485a1ecddd7103e9a