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Benzene, 1-iodo-4-(trifluoromethyl)- → 8-(3,5-Dimethyl-isoxazole-4-sulfonyl)-2-(4-trifluoromethyl-phenyl)-2,8-diaza-spiro[4.5]decan-1-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzene, 1-iodo-4-(trifluoromethyl)- | HCID 67993 | — |
| 反応物 | 8-(3,5-Dimethyl-isoxazole-4-sulfonyl)-2,8-diaza-spiro[4.5]decan-1-one | HCID 59577900 | — |
| 生成物 | 8-(3,5-Dimethyl-isoxazole-4-sulfonyl)-2-(4-trifluoromethyl-phenyl)-2,8-diaza-spiro[4.5]decan-1-one | HCID 59577920 | — |
反応手順
This material was prepared according to example 162 step B) from 8-(3,5-dimethyl-isoxazole-4-sulfonyl)-2,8-diaza-spiro[4.5]decan-1-one and 1-iodo-4-trifluoromethyl-benzene. Off white solid. MS (ESI): 458.13 MH+).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08329904B2 |
| 出典データセット | uspto-grants-2012_12 |
| ORD ID | ord-45d7240adedc49e6b7f52eee18687476 |
| 出典メモ | uspto-grants-2012_12 |