Iodoethanol → 4-[2,5-dimethyl-4-m-tolylethynyl-imidazol-1-yl]-1-(2-hydroxy-ethyl)-1H-pyridin-2-one
反応式
[CH3:1][C:2]1[N:3]([C:17]2[CH:22]=[CH:21][NH:20][C:19](=[O:23])[CH:18]=2)[C:4]([CH3:16])=[C:5]([C:7]#[C:8][C:9]2[CH:10]=[C:11]([CH3:15])[CH:12]=[CH:13][CH:14]=2)[N:6]=1.I[CH2:25][CH2:26][OH:27]>>[CH3:1][C:2]1[N:3]([C:17]2[CH:22]=[CH:21][N:20]([CH2:25][CH2:26][OH:27])[C:19](=[O:23])[CH:18]=2)[C:4]([CH3:16])=[C:5]([C:7]#[C:8][C:9]2[CH:10]=[C:11]([CH3:15])[CH:12]=[CH:13][CH:14]=2)[N:6]=1参加物
3
実験手順
The title compound, light brown solid, MS: m/e=348.2 (M+H+), was prepared in accordance with the general method of example 3 from 4-[2,5-dimethyl-4-m-tolylethynyl-imidazol-1-yl]-1H-pyridin-2-one and 2-iodoethanol.
出典と根拠
- ORDレコード
- ord-190045877b564ae5be74ba17028f1ece
- 出典データセット
- uspto-grants-2012_12
- 特許番号
- US08334287B2
反応ノート
読み込み中…