Acetyl chloride → N-[3-(4-Methyl-2-nitro-phenylsulfanyl)-phenyl]-acetamide
反応式
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][C:9]2[CH:10]=[C:11]([NH2:15])[CH:12]=[CH:13][CH:14]=2)=[C:4]([N+:16]([O-:18])=[O:17])[CH:3]=1.[C:19](Cl)(=[O:21])[CH3:20]>C(Cl)Cl>[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][C:9]2[CH:10]=[C:11]([NH:15][C:19](=[O:21])[CH3:20])[CH:12]=[CH:13][CH:14]=2)=[C:4]([N+:16]([O-:18])=[O:17])[CH:3]=1参加物
4
実験手順
The title compound was prepared using 3-(4-Methyl-2-nitro-phenylsulfanyl)-phenylamine (8.20 g, 31.50 mmol) and acetyl chloride (2.72 g, 34.65 mmol) dissolved in CH2Cl2. This was stirred at room temperature for 2 hrs at which time the title compound was collected by filtration (8.78 g, 92
後処理
- customThe title compound was prepared
- filtrationwas collected by filtration (8.78 g, 92
出典と根拠
- ORDレコード
- ord-60da73c7dbe445af8b93e8dfc971c12f
- 出典データセット
- uspto-grants-2012_12
- 特許番号
- US08338605B2
反応ノート
読み込み中…