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2,6,7-Trichloroquinoxaline → 4-[N-methyl-N-(6,7-dichloro-2-quinoxalinyl)amino]phenol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,6,7-Trichloroquinoxaline | HCID 10036978 | — |
| 反応物 | p-(N-methylamino)phenol sulfate | HCID 10198132 | — |
| 生成物 | 4-[N-methyl-N-(6,7-dichloro-2-quinoxalinyl)amino]phenol | HCID 13323142 | — |
反応手順
2,6,7-Trichloroquinoxaline was reacted with 4-(N-methylamino)phenol sulfate, following essentially the same procedure as that described in Example 1 Part (a), to give 4-[N-methyl-N-(6,7-dichloro-2-quinoxalinyl)amino]phenol. Proton magnetic resonance spectrum (d6 -acetone; δ in ppm): 8.25 (1H, s, quinoxaline hetero-ring proton); 8.0 (1H, s, quinoxaline benzo-ring proton); 7.9 (1H, s, quinoxaline benzo-ring proton); 7.15 (4H, m, phenoxy protons; 3.55 (3H, s, N-CH3).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04358307 |
| 出典データセット | uspto-grants-1982_11 |
| ORD ID | ord-e1d78a485c09482180c846166cea71b2 |
| 出典メモ | uspto-grants-1982_11 |