化工社化工社 化学情報印刷レポート · 研究参考用
2-Bromopropane → Cyclododecylmethyl-isopropyl-ether
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Bromopropane | HCID 6358 | — |
| 反応物 | Cyclododecanemethanol | HCID 74686 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Cyclododecylmethyl-isopropyl-ether | HCID 20519071 | — |
反応手順
According to the disclosure of Example 1, 99 g of hydroxymethylcyclododecane was first converted into the sodium alcoholate. 74 g (0.6 mol) of 2-bromopropane was added dropwise to the boiling suspension, and then the mixture was heated for 30 hours under reflux. The reaction mixture was poured into water, the organic phase was washed with water, dried over Na2SO4, and then distilled.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04359588 |
| 出典データセット | uspto-grants-1982_11 |
| ORD ID | ord-dcbf17b5baba4e33805706cfee481f0a |
| 出典メモ | uspto-grants-1982_11 |