tert-Butyl 6-bromoindoline-1-carboxylate → tert-butyl 6-allyl-2,3-dihydro-1H-indole-1-carboxylate
反応式
Br[C:2]1[CH:10]=[C:9]2[C:5]([CH2:6][CH2:7][N:8]2[C:11]([O:13][C:14]([CH3:17])([CH3:16])[CH3:15])=[O:12])=[CH:4][CH:3]=1.[CH3:18][C:19]1C=CC=C(C)[C:20]=1CN1C2C(=CC=C(C(O)=O)C=2)C=C1>>[CH2:20]([C:2]1[CH:10]=[C:9]2[C:5]([CH2:6][CH2:7][N:8]2[C:11]([O:13][C:14]([CH3:17])([CH3:16])[CH3:15])=[O:12])=[CH:4][CH:3]=1)[CH:19]=[CH2:18]参加物
3
実験手順
The titled compound (5.7 g) as a colorless oil was prepared from tert-butyl 6-bromo-2,3-dihydro-1H-indole-1-carboxylate (7.5 g) obtained with the method described in the document (WO 1998/43956 A) according to the method of the process (2) of Example 66.
後処理
- customobtained with the method
出典と根拠
- ORDレコード
- ord-8551fd4e07ec4aba9027f8178199fd95
- 出典データセット
- uspto-grants-2016_06
- 特許番号
- US09359350B2
反応ノート
読み込み中…