Hexamethyldisilazane → HCID 178504300、化合物

HRID 22000

反応式

HRID 22000 の反応式
[NH:1]1[CH:8]=[CH:7][C:5](N)=[N:4][C:2]1=[O:3].S([O-])([O-])(=O)=O.[NH4+].[NH4+].[CH3:16][Si:17]([CH3:24])([CH3:23])[NH:18][Si:19]([CH3:22])([CH3:21])[CH3:20]>>[CH3:16][Si:17]([N:18]([Si:19]([CH3:22])([CH3:21])[CH3:20])[C:8]1[CH:7]=[CH:5][NH:4][C:2](=[O:3])[N:1]=1)([CH3:24])[CH3:23]

参加物

4

反応物 3

HCID 13838HexamethyldisilazaneHCID 6097028Ammonium SulfateHCID 178418229Cytosine

生成物 1

HCID 178504300HCID 178504300、化合物

実験手順

Cytosine (12.0 g), hexamethyldisilazane (60 ml) and ammonium sulfate (10 mg) were refluxed at 125° C. for 30 minutes to form a homogenous solution. The hexamethyldisilazane was removed by distillation to form the titled product.

後処理

  1. customto form a homogenous solution
  2. customThe hexamethyldisilazane was removed by distillation

出典と根拠

ORDレコード
ord-d03adcd1c58a4cf4849e2f47f02abb57
出典データセット
uspto-grants-1995_06
特許番号
US05426183

関連ノート

読み込み中…