化工社化工社 化学情報印刷レポート · 研究参考用
Acetic Anhydride → N-(4-Fluoro-2-methylphenyl)acetamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic Anhydride | HCID 7918 | — |
| 反応物 | 4-Fluoro-2-methylaniline | HCID 67982 | — |
| 生成物 | N-(4-Fluoro-2-methylphenyl)acetamide | HCID 2737623 | 74% |
反応手順
A mixture of 4-fluoro-2-methylaniline (20 g) and (CH3CO)2O (400 mL) was stirred at RT for 3 hours. The reaction mixture was subsequently poured into ice water (1000 mL), stirred for 10 minutes, filtered, and dried under vacuum to give the title compound (20 g, 74%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09365566B2 |
| 出典データセット | uspto-grants-2016_06 |
| ORD ID | ord-259c4edab98645ea991b35ce6b268676 |
| 出典メモ | uspto-grants-2016_06 |