戻る
化工社化工社 化学情報印刷レポート · 研究参考用
HRID 2205252作成日:2026年10月27日

1,2-Dichloroethane → 1-(2-(2,3-Dimethylbut-2-en-1-yl)indolin-1-yl)ethanone

https://huagongshe.com/reaction/2205252

反応式

関与物質

役割名称HCID仕込み量
反応物1,2-DichloroethaneHCID 11—
反応物IndoleHCID 798—
反応物Tin tetrachlorideHCID 24287—
反応物3H-IndoleHCID 3083560—
反応物3,3,4-Trimethylpent-4-en-2-oneHCID 13262537—
生成物1-(2-(2,3-Dimethylbut-2-en-1-yl)indolin-1-yl)ethanoneHCID 7152587958%

反応手順

Following the general procedure as described in Example 11, 3,3,4-trimethylpent-4-en-2-one (0.50 g, 3.96 mmol), 1H-indole (0.56 g, 4.75 mmol) which was in situ isomerized to 3H-indole, and SnCl4 (1.24 g, 4.75 mmol) in 1,2-dichloroethane (40 ml) were reacted to give the title product as a white solid (0.56 g, 58%).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US09371262B2
出典データセットuspto-grants-2016_06
ORD IDord-cfeb19e361a74c21b17c8dd50fedbe70
出典メモuspto-grants-2016_06