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Pentanamide → N,N'-((4-(diethylamino)phenyl)methylene)dipentanamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Pentanamide | HCID 12298 | — |
| 反応物 | 4-(Diethylamino)benzaldehyde | HCID 67114 | — |
| 生成物 | N,N'-((4-(diethylamino)phenyl)methylene)dipentanamide | HCID 71451973 | 69% |
反応手順
Compound 52 was prepared from pentanamide and 4-(diethylamino)benzaldehyde using method 1. Yield: 69%. 1H NMR (400 MHz, CD3OD) δ 7.18 (d, J=8.8 Hz, 2H), 6.71 (d, J=8.8 Hz, 2H), 6.58 (t, J=8.4 Hz, 1H), 3.33-3.41 (m, 4H), 2.25 (t, J=7.2 Hz, 4H), 1.58-1.66 (m, 4H), 1.33-1.43 (m, 4H), 1.14 (t, J=7.2 Hz, 6H), 0.95 (t, J=2.8 Hz, 6H). LC-MS (ESI): m/z 362.2 (M+H)+. HRMS (ESI) for C21H36N3O2 (MH+): calcd, 362.2802. found 362.2792.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09376380B2 |
| 出典データセット | uspto-grants-2016_06 |
| ORD ID | ord-2749e43e622e4e3bb4738f309f0173bd |
| 出典メモ | uspto-grants-2016_06 |