関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 4-Coumaric acid | HCID 322 | — |
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | Glycidol | HCID 11164 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 溶媒 | Dimethyl Sulfoxide | HCID 679 | — |
| 溶媒 | Glycerol | HCID 753 | — |
| 生成物 | 2-Propenoic acid, 3-phenyl- | HCID 8784 | — |
反応手順
17.4 g of p-hydroxy cinnamic acid and 40.0 g of glycidol were dissolved in 20 ml of DMSO, and catalytic amount of sulfuric acid was added. The solution was heated to 90° C. and then heating and agitation was carried out for 3 hours, neutralized by adding sodium hydroxide and then adduct of cinnamic acid and glycerin was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05426210 |
|---|
| 出典データセット | uspto-grants-1995_06 |
|---|
| ORD ID | ord-9fd1cb87e984445880ac895829b5f575 |
|---|
| 出典メモ | uspto-grants-1995_06 |
|---|
