化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → 2-Propenoic acid, 3-phenyl-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | 4-Coumaric acid | HCID 322 | — |
| 反応物 | Nitrogen | HCID 947 | — |
| 反応物 | Glycidol | HCID 11164 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 溶媒 | Dimethyl Sulfoxide | HCID 679 | — |
| 溶媒 | Glycerol | HCID 753 | — |
| 生成物 | 2-Propenoic acid, 3-phenyl- | HCID 8784 | — |
反応手順
8.719 g of p-hydroxy cinnamic acid was dissolved in 10 ml of DMSO, and 100 mg of sodium hydroxide was added. The mixture was stirred and heated to 90° C. under a flow of N2 gas. 19.7 g of glycidol was added gradually, heating and agitation was carried out for 2 hours, neutralized by adding hydrochloric acid and then the adduct of cinnamic acid and glycerin was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05426210 |
| 出典データセット | uspto-grants-1995_06 |
| ORD ID | ord-b76ea8f01bb84b6080b39c1bfb6ab1c0 |
| 出典メモ | uspto-grants-1995_06 |