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Hydrochloric Acid → 2-Propenoic acid, 3-phenyl-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | 4-Coumaric acid | HCID 322 | — |
| 反応物 | Nitrogen | HCID 947 | — |
| 反応物 | Glycidol | HCID 11164 | — |
| 反応物 | Sodium | HCID 5360545 | — |
| 溶媒 | Dimethyl Sulfoxide | HCID 679 | — |
| 溶媒 | Glycerol | HCID 753 | — |
| 生成物 | 2-Propenoic acid, 3-phenyl- | HCID 8784 | — |
反応手順
2.8 g of p-hydroxy cinnamic acid was dissolved in 3 ml of DMSO, and 10 mg of sodium was added. The mixture was stirred and heated to 90° C. under a flow of N2 gas. 5.0 g of glycidol was added gradually, the heating and agitation was carried out for 1 hours, neutralized by adding hydrochloric acid and then the adduct of cinnamic acid and glycerin was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05426210 |
| 出典データセット | uspto-grants-1995_06 |
| ORD ID | ord-6b9e768bb16f4b5ebfd44303c1c7b17e |
| 出典メモ | uspto-grants-1995_06 |