2,2'-Bithiophene → 5-Bromo-2-chloro-1-(5-(2-thienyl)-2-thienylmethyl)benzene
反応式
[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6]1[S:7][CH:8]=[CH:9][CH:10]=1.[Br:11][C:12]1[CH:13]=[CH:14][C:15]([Cl:20])=[C:16]([CH:19]=1)[CH:17]=O>>[Br:11][C:12]1[CH:13]=[CH:14][C:15]([Cl:20])=[C:16]([CH2:17][C:5]2[S:1][C:2]([C:6]3[S:7][CH:8]=[CH:9][CH:10]=3)=[CH:3][CH:4]=2)[CH:19]=1参加物
3
実験手順
2,2′-Bithiophene and 5-bromo-2-chlorobenzaldehyde obtained in Reference Example 16-(1) were used and treated in a manner similar to Reference Example 9 to give the target compound. APCI-Mass m/Z 369/371 (M+H).
後処理
- additiontreated in a manner similar to Reference Example 9
- customto give the target compound
出典と根拠
- ORDレコード
- ord-01f892247f0946ec8d8ba4eba7b53094
- 出典データセット
- uspto-grants-2012_06
- 特許番号
- US08202984B2
反応ノート
読み込み中…