化工社化工社 化学情報印刷レポート · 研究参考用
1-Benzothiophene-2-carbaldehyde → 2-(4-Bromo-1-methoxynaphthalen-2-yl-methyl)benzo[b]thiophene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Benzothiophene-2-carbaldehyde | HCID 736500 | — |
| 反応物 | 2,4-Dibromo-1-methoxynaphthalene | HCID 3572059 | — |
| 生成物 | 2-(4-Bromo-1-methoxynaphthalen-2-yl-methyl)benzo[b]thiophene | HCID 66608193 | — |
反応手順
2,4-Dibromo-1-methoxynaphthalene (see J. Clayden, et al. Org. Lett., 5, (2003) 831) and benzo[b]thiophene-2-carboxaldehyde were treated in a manner similar to Reference Example 1 to give the target compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08202984B2 |
| 出典データセット | uspto-grants-2012_06 |
| ORD ID | ord-fa51ac3b14d642d0ae9bd0fbe47c9133 |
| 出典メモ | uspto-grants-2012_06 |