5-Methylbenzo(b)thiophene → 5-Bromo-2-chloro-1-(5-methylbenzo[b]thiophen-2-ylmethyl)benzene
反応式
[CH3:1][C:2]1[CH:10]=[CH:9][C:5]2[S:6][CH:7]=[CH:8][C:4]=2[CH:3]=1.[Br:11][C:12]1[CH:13]=[CH:14][C:15]([Cl:20])=[C:16]([CH:19]=1)[CH:17]=O>>[Br:11][C:12]1[CH:13]=[CH:14][C:15]([Cl:20])=[C:16]([CH2:17][C:7]2[S:6][C:5]3[CH:9]=[CH:10][C:2]([CH3:1])=[CH:3][C:4]=3[CH:8]=2)[CH:19]=1参加物
3
実験手順
5-Methylbenzo[b]thiophene and 5-bromo-2-chlorobenzaldehyde obtained in Reference Example 16-(1) were treated in a manner similar to Reference Example 7 to give the target compound.
後処理
- additionwere treated in a manner similar to Reference Example 7
- customto give the target compound
出典と根拠
- ORDレコード
- ord-0476b0ad28f2459a8640f9349c855d89
- 出典データセット
- uspto-grants-2012_06
- 特許番号
- US08202984B2
反応ノート
読み込み中…