3-Phenylpropyl 4-methylbenzenesulfonate → 3-Cyclohexylpropyl 4-methylbenzenesulfonate

HRID 2211075ノート

反応式

HRID 2211075 の反応式
C(C1CC2C(=CC=C(C3N=CC(O)=CN=3)C=2)C1)CCCCCCCCC.C(C1C=CC2N=C(C3C=CC(O)=CC=3)SC=2C=1)CCCCCCC.[C:51]1([CH3:70])[CH:56]=[CH:55][C:54]([S:57]([O:60][CH2:61][CH2:62][CH2:63][C:64]2[CH:69]=[CH:68][CH:67]=[CH:66][CH:65]=2)(=[O:59])=[O:58])=[CH:53][CH:52]=1>>[C:51]1([CH3:70])[CH:52]=[CH:53][C:54]([S:57]([O:60][CH2:61][CH2:62][CH2:63][CH:64]2[CH2:69][CH2:68][CH2:67][CH2:66][CH2:65]2)(=[O:59])=[O:58])=[CH:55][CH:56]=1

参加物

4

反応物 3

HCID 109899213-Phenylpropyl 4-methylbenzenesulfonateHCID 193753532-(2-Decylindan-5-yl)pyrimidine-5-olHCID 1360518844-(6-Octylbenzothiazole-2-yl)phenol

生成物 1

HCID 129566223-Cyclohexylpropyl 4-methylbenzenesulfonate収率 56.4%

実験手順

An objective product was prepared in the same manner as in Example 2 except that 2-(2-decylindan-5-yl)pyrimidine-5-ol was changed to 4-(6-octylbenzothiazole-2-yl)phenol and 3-phenylpropyl p-toluenesulfonate was changed to 3-cyclohexylpropyl p-toluenesulfonate (Yield: 56.4%).

出典と根拠

ORDレコード
ord-90fdaaa0f8eb4046bf314bbde8c31ad9
出典データセット
uspto-grants-1995_10
特許番号
US05462694

反応ノート

読み込み中…