3-Phenylpropyl 4-methylbenzenesulfonate → 3-Cyclohexylpropyl 4-methylbenzenesulfonate

HRID 2211077ノート

反応式

HRID 2211077 の反応式
C(C1CC2C(=CC=C(C3N=CC(O)=CN=3)C=2)C1)CCCCCCCCC.C(C1SC(C2C=CC(O)=CC=2)=NC=1)CCCCCCCCC.[C:49]1([CH3:68])[CH:54]=[CH:53][C:52]([S:55]([O:58][CH2:59][CH2:60][CH2:61][C:62]2[CH:67]=[CH:66][CH:65]=[CH:64][CH:63]=2)(=[O:57])=[O:56])=[CH:51][CH:50]=1>>[C:49]1([CH3:68])[CH:50]=[CH:51][C:52]([S:55]([O:58][CH2:59][CH2:60][CH2:61][CH:62]2[CH2:67][CH2:66][CH2:65][CH2:64][CH2:63]2)(=[O:57])=[O:56])=[CH:53][CH:54]=1

参加物

4

反応物 3

HCID 109899213-Phenylpropyl 4-methylbenzenesulfonateHCID 193753532-(2-Decylindan-5-yl)pyrimidine-5-olHCID 1355884184-(5-Decylthiazole-2-yl)phenol

生成物 1

HCID 129566223-Cyclohexylpropyl 4-methylbenzenesulfonate収率 25.6%

実験手順

An objective product was prepared in the same manner as in Example 2 except that 2-(2-decylindan-5-yl)pyrimidine-5-ol was changed to 4-(5-decylthiazole-2-yl)phenol and 3-phenylpropyl p-toluenesulfonate was changed to 3-cyclohexylpropyl p-toluenesulfonate (Yield: 25.6%).

出典と根拠

ORDレコード
ord-218964cf9ff04eba8770647f0410868b
出典データセット
uspto-grants-1995_10
特許番号
US05462694

反応ノート

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