関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | 1,5-Dimethoxy-2,4-dinitrobenzene | HCID 615053 | — |
| 溶媒 | N-methyl-2-pyrrolidone | HCID 13387 | — |
| 生成物 | 4,6-Dinitroresorcinol | HCID 61158 | 95% |
反応手順
A 100 mL, 3-necked, round-bottom flask is charged with 30 mL of N-methylpyrrolidinone, 2.6 g (0.02 mole) of 1,3-dimethoxy-4,6-dinitrobenzene. The resulting solution is heated to 130° C. for two to three hours. The reaction mixture is then cooled and poured into an excess of dilute hydrochloric acid. The resulting solid is isolated by filtration to yield 1.9 g (95% yield) of 4,6-dinitroresorcinol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05463129 |
|---|
| 出典データセット | uspto-grants-1995_10 |
|---|
| ORD ID | ord-ee69f858690d47bab1c6767ca626beb8 |
|---|
| 出典メモ | uspto-grants-1995_10 |
|---|
