Benzyl chloromethyl ether → tert-Butyl 4-[(benzyloxy)methyl]hexahydro-2-methylene-3-oxo-1,4-diazepine-1-carboxylate

HRID 2211848

反応式

HRID 2211848 の反応式
[CH2:1]([O:8][CH2:9][N:10]1[CH2:16][CH2:15][CH2:14][N:13]([C:17]([O:19][C:20]([CH3:23])([CH3:22])[CH3:21])=[O:18])[CH2:12][C:11]1=[O:24])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Cl[CH2:26]OCC1C=CC=CC=1>>[CH2:1]([O:8][CH2:9][N:10]1[CH2:16][CH2:15][CH2:14][N:13]([C:17]([O:19][C:20]([CH3:21])([CH3:23])[CH3:22])=[O:18])[C:12](=[CH2:26])[C:11]1=[O:24])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

参加物

3

反応物 2

HCID 137983Benzyl chloromethyl etherHCID 21962085tert-Butyl 4-[(Benzyloxy)methyl]hexahydro-3-oxo-1H-1,4-diazepine-1-carboxylate

生成物 1

HCID 21962090tert-Butyl 4-[(benzyloxy)methyl]hexahydro-2-methylene-3-oxo-1,4-diazepine-1-carboxylate

実験手順

The title was prepared from tert-butyl 4-[(benzyloxy)methyl]hexahydro-3-oxo-1H-1,4-diazepine-1-carboxylate and benzyl chloromethyl ether essentially following the procedure described in Example 3, Step 1.

出典と根拠

ORDレコード
ord-c4d802a4e54a4056b84e1ba1c27b7cf7
出典データセット
uspto-grants-2006_09
特許番号
US07101871B2

関連ノート

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