HCID 131728098、化合物 → 2-Sulfanylundecanoic acid

HRID 221185ノート

反応式

HRID 221185 の反応式
[SH:1][CH:2]([CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14])[C:3]([OH:5])=[O:4].CO>[Se-2].[Cd+2]>[SH:1][CH:2]([CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14])[C:3]([OH:5])=[O:4]

参加物

3

反応物 1

HCID 131728098HCID 131728098、化合物

生成物 1

HCID 219323062-Sulfanylundecanoic acid

試薬・触媒・溶媒 1

HCID 9837007Cadmium monoselenide溶媒

実験手順

In the absence of light, the precipitated CdSe nanocrystals are dissolved in the MUA-methanol solution. The resulting solution is stirred under an Argon flow for about 2 hours to form mercaptoundecanoic acid (MUA)-capped CdSe nanocrystals. Ethyl acetate and ethyl ether are used to precipitate and wash (repeatedly between about 2 and 3 times) the MUA-capped CdSe nanocrystals. Subsequently, the MUA-capped CdSe nanocrystals preferably are dispersed in isopropanol to define a cadmium selenide (CdSe) solution.

出典と根拠

ORDレコード
ord-b80ea75d1a654cc59ecbbeb9f1e5f6b8
出典データセット
uspto-grants-2012_06
特許番号
US08206824B2

反応ノート

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