Aniline → HCID 66664557、化合物

HRID 221314

反応式

HRID 221314 の反応式
F[C:2]1C=CC=C2C=1C(=O)N(C1C=CC=CC=1)C([C@@H](NC1N=CN=C3C=1N=CN3)CC)=N2.[N+:32]([C:35]1[CH:43]=[CH:42][C:41](C)=[CH:40][C:36]=1[C:37]([OH:39])=O)([O-:34])=[O:33].FC1C=CC=C([N+]([O-])=O)C=1C(O)=O.[F:58][C:59]1[CH:65]=[CH:64][CH:63]=[C:62]([F:66])[C:60]=1[NH2:61].NC1C=CC=CC=1>>[F:58][C:59]1[CH:65]=[CH:64][CH:63]=[C:62]([F:66])[C:60]=1[NH:61][C:37](=[O:39])[C:36]1[C:35]([N+:32]([O-:34])=[O:33])=[CH:43][CH:42]=[CH:41][C:40]=1[CH3:2]

参加物

6

反応物 5

HCID 6115AnilineHCID 183715-Methyl-2-nitrobenzoic acidHCID 796472,6-DifluoroanilineHCID 6037582-Fluoro-6-nitrobenzoic acidHCID 178456065HCID 178456065、化合物

生成物 1

HCID 66664557HCID 66664557、化合物

実験手順

Compound 118a was prepared following the preparation procedure described above with respect to compound 107, but 2-nitro-5-methylbenzoic acid was substituted for 2-fluoro-6-nitrobenzoic acid and 2,6-difluoroaniline was substituted for aniline.

後処理

  1. customthe preparation procedure

出典と根拠

ORDレコード
ord-d59e7ee8af924843bc6ac5f7c6917486
出典データセット
uspto-grants-2012_06
特許番号
US08207153B2

関連ノート

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