2,6-Diisopropylphenyl isocyanate → N'-(2,6-diisopropylphenyl)-N-[(4-dimethylaminophenyl)methyl]-N-(4-ethylphenyl)urea

HRID 2213624

反応式

HRID 2213624 の反応式
[CH3:1][N:2]([CH3:19])[C:3]1[CH:8]=[CH:7][C:6]([CH2:9][NH:10][C:11]2[CH:16]=[CH:15][C:14]([CH2:17][CH3:18])=[CH:13][CH:12]=2)=[CH:5][CH:4]=1.[CH:20]([C:23]1[CH:28]=[CH:27][CH:26]=[C:25]([CH:29]([CH3:31])[CH3:30])[C:24]=1[N:32]=[C:33]=[O:34])([CH3:22])[CH3:21]>>[CH:20]([C:23]1[CH:28]=[CH:27][CH:26]=[C:25]([CH:29]([CH3:30])[CH3:31])[C:24]=1[NH:32][C:33](=[O:34])[N:10]([CH2:9][C:6]1[CH:5]=[CH:4][C:3]([N:2]([CH3:19])[CH3:1])=[CH:8][CH:7]=1)[C:11]1[CH:16]=[CH:15][C:14]([CH2:17][CH3:18])=[CH:13][CH:12]=1)([CH3:21])[CH3:22]

参加物

3

反応物 2

HCID 922592,6-Diisopropylphenyl isocyanateHCID 3482181[(4-Dimethylaminophenyl)methyl](4-ethylphenyl)amine

生成物 1

HCID 10139273N'-(2,6-diisopropylphenyl)-N-[(4-dimethylaminophenyl)methyl]-N-(4-ethylphenyl)urea収率 57.2%

実験手順

By the reaction and treatment in the same manner as in Example 2 using [(4-dimethylaminophenyl)methyl](4-ethylphenyl)amine (0.70 g) and 2,6-diisopropylphenyl isocyanate (0.68 g) as starting materials, N′-(2,6-diisopropylphenyl)-N-[(4-dimethylaminophenyl)methyl]-N-(4-ethylphenyl)urea (0.72 g) was obtained.

出典と根拠

ORDレコード
ord-cf077fbfb71946f899b2f956df345804
出典データセット
uspto-grants-2006_09
特許番号
US07105567B2

関連ノート

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