反応式
[CH:1]#[C:2][CH2:3][CH2:4]CC.[C:7]1([C:13]#[CH:14])[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1.C(#N)C1C=CC=CC=1>>[C:13]([C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)#[C:14][CH2:1][CH2:2][CH2:3][CH3:4]参加物
4
実験手順
The procedure was identical to Example 1, with the exception that 1-hexyne (0.450 ml; 0.329 g; 4.00 mmol) was used as a substrate instead of phenylacetylene. GC analysis of the organic phase of the hydrolyzed reaction sample after 20 h at 65° C. showed the presence of 1.90 mmol (95% yield) of 1-hexynylbenzene and and 0.08 mmol of benzonitrile remaining in the reaction mixture.
出典と根拠
- ORDレコード
- ord-585442bfbe2140c0afdecb052599d445
- 出典データセット
- uspto-grants-2006_09
- 特許番号
- US07105707B2
関連ノート
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