化工社化工社 化学情報印刷レポート · 研究参考用
N,N,N',N',N'',N''-Hexamethylmethanetriamine → 2-Di-n-propylamino-8-(1-oxo-2-methoxy-3-(dimethylamino)-prop-2-enyl)-1,2,3,4-tetrahydronaphthalene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N,N,N',N',N'',N''-Hexamethylmethanetriamine | HCID 79831 | — |
| 反応物 | 2-Di-n-propylamino-8-methoxyacetyl-1,2,3,4-tetrahydronaphthalene | HCID 15233538 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | 2-Di-n-propylamino-8-(1-oxo-2-methoxy-3-(dimethylamino)-prop-2-enyl)-1,2,3,4-tetrahydronaphthalene | HCID 54314453 | — |
反応手順
A solution of 2-di-n-propylamino-8-methoxyacetyl-1,2,3,4-tetrahydronaphthalene (1.0 g) and tris(dimethylamino)methane (1.5 ml) in toluene (25 ml) was heated to reflux for 1.5 hours. The reaction was concentrated to give crude 2-di-n-propylamino-8-(1-oxo-2-methoxy-3-(dimethylamino)-prop-2-enyl)-1,2,3,4-tetrahydronaphthalene (1.2 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05426226 |
| 出典データセット | uspto-grants-1995_06 |
| ORD ID | ord-d69cbf67c5e94511b5896dc70085b5e5 |
| 出典メモ | uspto-grants-1995_06 |