HCID 11788638、化合物 → HCID 21055355、化合物
反応式
[NH2:1][C@H:2]1[CH2:8][S:7][C:6]2[CH:9]=[CH:10][CH:11]=[CH:12][C:5]=2[O:4][CH2:3]1.O[C:14]1C=CC(C)=CC=1S>>[NH2:1][C@H:2]1[CH2:8][S:7][C:6]2[CH:9]=[C:10]([CH3:14])[CH:11]=[CH:12][C:5]=2[O:4][CH2:3]1参加物
3
実験手順
The title compound (Ib) is prepared according to a reaction sequence identical to that employed for the synthesis of 3-(R)-amino-3,4-dihydro-2H-1,5-benzoxathiepine (Ia-1) but using, as starting material, 2-hydroxy-5-methylthiophenol (IVb) instead of 2-hydroxythiophenol. The title compound (Ib) is obtained in the form of a yellow oil.
後処理
- customThe title compound (Ib) is prepared
出典と根拠
- ORDレコード
- ord-f3f0d9c83f3149908bba3a0878dc450c
- 出典データセット
- uspto-grants-2006_09
- 特許番号
- US07109234B2
反応ノート
読み込み中…