Triethylamine → HCID 86590086、化合物
反応式
[O:1]1[C:5]([C:6]([OH:8])=O)=[CH:4][C:3]2[CH:9]=[CH:10][CH:11]=[CH:12][C:2]1=2.Cl.N[C:15]1[CH:16]=[CH:17][C:18]([O:23][CH2:24][C:25]([CH3:29])([CH3:28])[CH2:26][OH:27])=[C:19]([CH:22]=1)[C:20]#[N:21].C([N:32](CC)CC)C>>[C:20]([C:19]1[CH:22]=[C:15]([C:4]2[C:3]3[CH:9]=[CH:10][CH:11]=[CH:12][C:2]=3[O:1][C:5]=2[C:6]([NH2:32])=[O:8])[CH:16]=[CH:17][C:18]=1[O:23][CH2:24][C:25]([CH3:28])([CH3:29])[CH2:26][OH:27])#[N:21]参加物
4
実験手順
By the reaction and treatment in the same manner as in Example 6 using benzo[b]furan-2-carboxylic acid (0.7 g), 5-amino-2-(2,2-dimethyl-3-hydroxypropoxy)benzonitrile monohydrochloride (1.0 g) and triethylamine (0.6 ml), the title compound (0.26 g) was obtained. melting point: 199-201° C.
出典と根拠
- ORDレコード
- ord-303cbd8d013844e89f7a6cfa3f83c3b9
- 出典データセット