Ammonium Chloride → HCID 178425624、化合物
反応式
[CH3:1][C:2]1([CH3:10])[CH2:7][CH2:6][C:5](OC)=[N:4][CH2:3]1.[Cl-:11].[NH4+:12]>C(O)C>[ClH:11].[CH3:1][C:2]1([CH3:10])[CH2:3][NH:4][C:5](=[NH:12])[CH2:6][CH2:7]1参加物
4
実験手順
The mixture of 3,3-dimethyl-6-methoxy-2,3,4,5-tetrahydropyridine (9.0 g, 64 mmol) and ammonium chloride (3.4 g, 64 mmol) in dry ethanol (160 mL) was heated to reflux for 2 h. The reaction mixture was then concentrated under reduced pressure and the titled compound was obtained as a white solid (9.9 g, 94.6%).
後処理
- temperaturewas heated
- temperatureto reflux for 2 h
- concentrationThe reaction mixture was then concentrated under reduced pressure
出典と根拠
- ORDレコード
- ord-32014185ff6946bea573072723556ba0
- 出典データセット
- uspto-grants-2006_09
- 特許番号
- US07112582B2
反応ノート
読み込み中…